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Effects of heat treatment on the properties of powder injection molded AIN ceramics Effects of heat treatment on the properties of powder injection molded AIN ceramics

Effects of heat treatment on the properties of powder injection molded AIN ceramics

  • 期刊名字:稀有金屬
  • 文件大?。?/li>
  • 論文作者:DU Xueli,QIN Mingli,Akhtar Far
  • 作者單位:Institute of Powder Metallurgy,School of Materials Science and Engineering
  • 更新時(shí)間:2023-02-07
  • 下載次數(shù):
論文簡介

The effects of two different heat-treatment atmospheres,nitrogen atmosphere and reducing nitrogen atmosphere with carbon,on the properties of Y2O3-doped aluminum nitride (AlN) ceramics were investigated.The AlN powder as a raw material was synthesized by self-propagating high-temperature synthesis (SHS) and compacts were fabricated by employing powder injection molding technique.The polymer-wax binder consisted of 60 wt.% paraffin wax (PW),35 wt.% polypropylene (PP),and 5 wt.% stearic acid (SA).After the removal of binder,specimens were sintered at 1850℃ in nitrogen atmosphere under atmospheric pressure.To improve the thermal conductivity,sintered samples were reheated.The result reveals that the heat-treatment atmosphere has significant effect on the properties and secondary phase of AlN ceramics.The thermal conductivity and density of AlN ceramics reheated in nitrogen gas are 180 W·m-1 K-1 and 3.28 g,cm-3 and the secondary phase is yttrium aluminate.For the sample reheated in reducing nitrogen atmosphere with carbon,the thermal conductivity and density are 173 W.m-1.K-1 and 3.23 g·cm-3,respectively,and the secondary phase is YN.

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